Solid state NMR

Cover of: Solid state NMR |

Published by Springer-Verlag in Berlin, New York .

Written in English

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Subjects:

  • Nuclear magnetic resonance spectroscopy

Edition Notes

Includes bibliographical references and indexes.

Book details

Statementguest-editor, B. Blümich.
SeriesNMR ;, 30-33, 35, NMR (Series) ;, v. 30-33, 35.
ContributionsBlümich, Bernhard., Born, R., Spiess, Hans Wolfgang, 1942-
Classifications
LC ClassificationsQC490 .N2 vol. 30, etc.
The Physical Object
Pagination5 v. :
ID Numbers
Open LibraryOL1401628M
ISBN 103540571892, 0387571892
LC Control Number93009522
OCLC/WorldCa29967472

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In this concise introduction to the growing field of solid-state nuclear magnetic resonance spectroscopy, the reader will find: * Basic NMR concepts for solids, including guidance on the spin-1/2 nuclei concept * Coverage of the quantum mechanics aspects of solid state NMR and an introduction to the concept of quadrupolar nuclei * An 5/5(1).

Introduction to Solid State NMR Spectroscopy is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solid-state nuclear magnetic resonance spectroscopy or undertaking research projects where solid-state NMR is likely to be a major investigative technique.

It will also serve as a practical introduction in industry, where the techniques can provide Cited by: Solid State NMR Spectroscopy, by Melinda Duer Middle level Publisher webpage for this bookThis is a good middle level book on a number of SSNMR topics, with a detail level that works well for a year graduate student.

The book cover links to the publishers website, however copies of this book are available for a cheaper price on other. Book chapter Full text access Chapter Six - Solid-state NMR studies on crystalline Solid state NMR book polymer electrolytes and important cathode materials for lithium-ion batteries Fushan Geng.

Solid-State NMR IV, Methods and Applications of Solid-State NMR in NMR Basic Principles and Progress, Vol. 33 Bernhard Blümich (Ed.), Springer-Verlag, Berlin (). Multidimensional Solid-State NMR and Polymers, Klaus Schmidt-Rohr and Hans Wolfgang Spiess, Academic, London ().

Nuclear Magnetic Resonance Probes of Molecular Dynamics. Introduction to Solid State NMR In solution NMR, spectra consist of a series of very sharp transitions, due to averaging of anisotropic NMR interactions by rapid random tumbling.

By contrast, solid-state NMR spectra are very broad, as the full effects of anisotropic or orientation-dependent interactions are observed in the spectrum. This book is for those familiar with solution-state NMR who are encountering solid-state NMR for the first time.

It presents the current understanding and applications of solid-state NMR with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details.

This dual requirement is met through careful construction of 4/5(1). NMR has made important contributions to our understanding of structure–property relationships in polymers. This book provides an up-to-date and comprehensive overview of the fundamentals of NMR, with applications of multidimensional NMR and the new.

ISBN: OCLC Number: Description: xi, pages: illustrations: Contents: Dipolar recoupling / Niels Chr. Nielsen, Lasse A Strassø, and Anders B. Nielsen --Solid-state NMR techniques for the structural determination of amyloid fibrils / Jerry C.C. Chan --Solid-state (B9F-NMR of peptides in native membranes / Katja Koch, Sergii.

Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods.

Dipolar Recoupling, by Niels Chr. Nielsen, Lasse A. Strassø and Anders B. Nielsen.-Solid-State NMR Techniques for the Structural Determination of Amyloid Fibrils, by Jerry C. Chan.-Solid-State 19F-NMR of Peptides in Native Membranes, by Katja Koch, Sergii Afonin, Marco Ieronimo, Marina Berditsch.

With additional coverage of the practical implementation of solid-state NMR experiments integrated into the discussion, this book will Solid state NMR book essential reading for all those using, or about to use, solid-state NMR spectroscopy.

Dr Melinda Duer is a senior lecturer in the Department of Chemistry at the University of Cambridge, Cambridge, : Melinda J. Duer. Solid state NMR spectroscopy is a powerful method in many research areas: Batteries In semi-ordered or ordered materials, such as batteries, important transport processes can be measured.

Measuring the charge transport in batteries can help understand the reason for its conductivity. The NOOK Book (eBook) of the Solid State NMR of Polymers by T.

Asakura at Barnes & Noble. FREE Shipping on $35 or more. Due to COVID, orders may be delayed. Thank you for your patience. Book Annex Membership Educators Gift Cards Stores & Events Help Auto Suggestions are available once you type at least 3 letters. Pages: About this book. Solid-state NMR covers an enormous range of material types and experimental techniques.

Although the basic instrumentation and techniques of solids NMR are readily accessible, there can be significant barriers, even for existing experts, to exploring the bewildering array of more sophisticated techniques. The book is divided into two parts: "Fundamentals" and "Further Applications." The section on Fundamentals contains relatively long chapters that deal with the basic theory and practice of solid-state NMR.

The essential differences and extra scope of solid-state NMR over solution-state is dealt with in an introductory chapter. NMR spectroscopy is the most valuable and versatile analytical tool in chemistry.

While excellent monographs exist on high-resolution NMR in liquids and solids, this is the first book to address multidimensional solid-state NMR. The journal Solid State Nuclear Magnetic Resonance publishes original manuscripts of high scientific quality dealing with all experimental and theoretical aspects of solid state NMR.

This includes advances in instrumentation, development of new experimental techniques and methodology, new theoretical insights, new data processing and simulation.

This book is Volume in the series ‘Lecture Notes in Chemistry’ published by Springer. It can be organised into three sections: (a) principles of NMR theory (Chapter 1); (b) solid-state NMR studies of zeolites and related materials (Chapters 2 and 3); and (c) surface chemistry and reaction chemistry over zeolites (Chapters 4–6).

This book provides a comprehensive account of state-of-the-art solid-state NMR techniques and the application of these techniques in heterogeneous catalysts and related catalytic reactions, which is suitable as a reference guide for both experienced researchers in and newcomers.

With additional coverage of the practical implementation of solid-state NMR experiments integrated into the discussion, this book will be essential reading for all those using, or about to use, solid-state NMR spectroscopy.

Dr Melinda Duer is a senior lecturer in the Department of Chemistry at the University of Cambridge, Cambridge, UK. Solid-state NMR now favorably competes with well-established techniques, such as light, x-ray, or neutron scattering, electron microscopy, and dielectric and mechanical relaxation.

Part of a multi-volume work on solid-state nuclear magnetic resonance imaging, this particular volume covers solid-state NMR line narrowing methods for quadrupolar nuclei, structural studies of Read more.

CHAPTER 14 - SOLID-STATE NMR SPECTROSCOPY SUMMARY Experiment - Shimming Solid-State Probe-Heads Experiment – Adjusting the Magic Angle Experiment - Hartmann-Hahn Matching Experiment – The Basic CP/MAS Experiment Experiment - TOSS Experiment - SELTICS Solid-state NMR is able to provide us with a wealth of information on the physical and chemical state of pharmaceutical products at every stage of drug development.

It is a highly sensitive technique, able to identify crystalline and amorphous forms of drugs and excipients, as well as solvates and hydrates. @article{osti_, title = {High-resolution solid-state NMR of silicates and zeolites}, author = {Engelhardt, G and Michel, D}, abstractNote = {Although the basic principles and methods of high-resolution solid-state NMR are presented in this volume, the emphasis is on applications.

References are extensive and include material published in. Hence solid-state NMR is a field in itself, separate from solution-state NMR, and is generally considered more difficult. Which is why it is not as routine as solution state nmr. This book finds a good balance, offering an excellent starting point for your first (and second) step into solid state NMR.

The book first considers different types of solids and their. Asked to answer, so I’ll jump in here. Kittel is probably the most popular out there. I don’t like it as much, though, because in my opinion Kittel’s style is a bit terse in that he doesn’t provide as much detail into deriving the equations as I’d.

Solid‐state NMR Lineshapes The Orientational Dependence of the NMR Resonance Frequency. Single‐crystal NMR. Powder Spectra. One‐dimensional 2 H NMR Magic‐angle Spinning CP MAS NMR.

1 H Solid‐State NMR Recoupling Methods. Solid-State NMR Techniques for the Structural Determination of Amyloid Fibrils, by Jerry C. Chan.-Solid-State 19 F-NMR of Peptides in Native Membranes, by Katja Koch, Sergii Afonin, Marco Ieronimo, Marina Berditsch and Anne S.

Ulrich It includes an introduction to the basic theory of solid-state NMR and various frequently used techniques. Special emphasis is placed on characterizing the framework and pore structure, active site, guest-host interaction, and synthesis mechanisms of heterogeneous catalysts using multinuclear one- and two-dimensional solid-sate NMR spectroscopy.

Summary. Solid-state NMR is a powerful physical method widely applied in modern fundamental and applied science, medicine, and industry.

Its role is particularly valuable in materials chemistry due to the capability of solid-state NMR to rapidly solve tasks connected with structural descriptions of complex systems on macro and/or molecular levels, and the identification of the dynamics often. Introduction to Solid State NMR Spectroscopy is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solid-state nuclear magnetic resonance spectroscopy or undertaking research projects where solid-state NMR is likely to be a major investigative technique.

It will also serve as a practical introduction in industry, where the techniques can provide Price: $   Solid-State NMR Techniques for the Structural Determination of Amyloid Fibrils, by Jerry C.

Chan.-Solid-State 19F-NMR of Peptides in Native Membranes, by Katja Koch, Sergii Afonin, Marco Ieronimo, Marina Berditsch and Anne S. Ulrich.-Brand: Springer Berlin Heidelberg.

Solid state NMR is a powerful, but subtle, technique for the characterisation of solid materials. It is strongly complementary to diffraction-based techniques (which are sensitive to long-range ordering) in that it probes local chemical environments and so can be applied successfully to all manner of materials whether crystalline or not, homogeneous or not.

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Solid-state NMR spectra generally reflect the sum of several independent interactions such as Zeeman, dipolar and quadrupolar coupling as well as magnetic shielding effects.

To obtain the desired information, separation of these effects and their decoding is essential. Buy Solid-State NMR: Basic Principles and Practice by David C Apperley, Robin K Harris, Paul Hodgkinson (ISBN: ) from Amazon's Book Store. Everyday low prices and free delivery on eligible s: 3.

Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods. This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods.

High-resolution solid-state NMR has recently been extensively applied to study structure and solid-state reactions of inorganic silicates, aluminosilicates and, in particular, zeolites. In addition, a variety of NMR methods including conventional FT NMR techniques have been successfully used to investigate sorbate-sorbent interactions and the.Solid-state chemistry, also sometimes referred as materials chemistry, is the study of the synthesis, structure, and properties of solid phase materials, particularly, but not necessarily exclusively of, non-molecular therefore has a strong overlap with solid-state physics, mineralogy, crystallography, ceramics, metallurgy, thermodynamics, materials science and electronics with a.Solid-state NMR Spectroscopy - An Introduction Rene Verel [email protected] HCI D Outline General Principles of NMR Spectroscopy Interactions relevant to NMR Spectroscopy (and their information content) Differences between solution and solid state NMR .

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